The loss dropped the Tigerettes to 15-8 on the season.
Ashtin Zamzow led Goliad with 15 kills and Roxanne Morris added 12. Sydney Morris had 21 digs, while Zamzow added 14 and Roxanne Morris had 12.
Kendall Coles topped the Tigerettes in assists with 21 and Zamzow added 12.
Goliad will return to Tuesday in a District 30-2A match at Bloomington and will play at Edna on Friday.